Position |
IVM |
IVM |
M1 |
M1 |
M3 |
M3 |
|
H shift [ppm] |
C shift [ppm] |
H shift [ppm] |
C shift
[ppm] |
H shift [ppm] |
C shift [ppm] |
1 |
- |
171.91 |
- |
171.98 |
- |
171.72 |
2 |
3.16 |
45.61 |
3.19 |
45.67 |
3.25 |
45.53 |
3 |
5.42 |
118.65 |
5.42 |
118.60 |
5.70 |
118.64 |
4 |
- |
136.50 |
- |
136.69 |
- |
139.78 |
5 |
4.19 |
67.47 |
4.20 |
67.43 |
4.41 |
65.22 |
6 |
3.78 |
80.37 |
3.79 |
80.31 |
3.81 |
80.48 |
7 |
- |
80.48 |
- |
80.47 |
- |
80.79 |
8 |
- |
140.36 |
- |
140.37 |
- |
140.28 |
9 |
5.84 |
120.29 |
5.84 |
120.33 |
5.86 |
120.55 |
10 |
5.89 |
125.16 |
5.89 |
125.15 |
5.90 |
125.18 |
11 |
5.81 |
137.39 |
5.80 |
137.56 |
5.81 |
137.68 |
12 |
2.63 |
39.44 |
2.63 |
39.52 |
2.64 |
39.55 |
13 |
3.96 |
81.74 |
3.96 |
81.72 |
3.96 |
39.55 |
14 |
- |
134.84 |
- |
134.81 |
- |
134.85 |
15 |
5.21 |
118.89 |
5.21 |
118.98 |
5.22 |
118.94 |
16 (a/b) |
2.31/2.24 |
33.74 |
2.31/2.25 |
33.56 |
2.32/2.25 |
33.68 |
17 |
3.73 |
67.42 |
3.74 |
67.40 |
3.74 |
67.35 |
18 (a/b) |
1.9/0.79 |
36.50 |
1.91/0.80 |
36.51 |
1.91/0.80 |
36.55 |
19 |
5.04 |
68.55 |
5.07 |
68.44 |
5.09 |
68.60 |
20 (a/b) |
2.09/1.25 |
41.46 |
2.09/1.26 |
41.40 |
2.10/1.27 |
41.42 |
21 |
- |
97.43 |
- |
97.41 |
- |
97.46 |
22 (a/b) |
1.61/1.52 |
35.50 |
1.60/1.52 |
35.66 |
1.61/1.52 |
35.72 |
23 (a/b) |
1.53/1.52 |
27.99 |
1.53/1.52 |
27.90 |
1.53/1.52 |
27.99 |
24 |
1.54 |
31.10 |
1.54 |
31.07 |
1.54 |
31.09 |
25 |
3.29 |
76.19 |
3.30 |
76.28 |
3.30 |
76.23 |
26 (a/b) |
4.60/4.61 |
67.54 |
4.61/4.62 |
67.62 |
4.63/4.62 |
67.66 |
CH3/CH2 (a/b) (4) |
1.81 |
18.79 |
1.82 |
18.75 |
4.16/4.15 |
62.53 |
CH3 (12) |
1.16 |
19.68 |
1.16 |
19.62 |
1.17 |
19.63 |
CH3 (14) |
1.53 |
14.13 |
1.53 |
14.04 |
1.54 |
14.12 |
CH3 (24) |
0.81 |
16.72 |
0.82 |
16.63 |
0.82 |
16.72 |
27 |
1.62 |
35.22 |
1.62 |
35.17 |
1.63 |
35.22 |
CH3 (27) |
0.97 |
11.74 |
0.89 |
11.62 |
0.89 |
11.63 |
28 (a/b) |
1.56/1.40 |
27.03 |
1.56/1.41 |
27.03 |
1.57/1.41 |
27.01 |
CH3 (28) |
0.89 |
11.69 |
0.97 |
11.65 |
0.98 |
11.67 |
1´ |
4.78 |
94.89 |
4.79 |
94.81 |
4.79 |
94.90 |
2´ (a/b) |
2.30/1.51 |
34.31 |
2.30/1.53 |
34.07 |
2.29/1.53 |
34.22 |
3´ |
3.62 |
79.34 |
3.62 |
79.45 |
3.62 |
79.30 |
4´ |
3.18 |
80.13 |
3.18 |
80.15 |
3.19 |
80.25 |
5´ |
3.83 |
67.14 |
3.83 |
67.05 |
3.84 |
67.15 |
CH3 (3´) |
3.37 |
55.74 |
3.37 |
55.69 |
3.38 |
55.57 |
CH3 (5´) |
1.23 |
17.95 |
1.24 |
17.92 |
1.24 |
17.98 |
1´´ |
5.34 |
98.04 |
5.31 |
97.95 |
5.34 |
98.08 |
2´´ (a/b) |
2.26/1.46 |
34.55 |
2.07/1.59 |
38.02 |
2.27/1.47 |
34.69 |
3´´ |
3.33 |
78.05 |
3.64 |
68.43 |
3.35 |
78.06 |
4´´ |
3.01 |
76.01 |
2.92 |
77.70 |
3.02 |
76.14 |
5´´ |
3.66 |
68.42 |
3.67 |
68.44 |
3.68 |
68.45 |
CH3 (3´´) |
3.38 |
56.09 |
- |
- |
3.38 |
56.27 |
CH3 (5´´) |
1.20 |
17.11 |
1.20 |
17.01 |
1.20 |
17.08 |